24dB is an awful lot of gain for a preamp. 26dB is sort of a surprisingly high gain for a 30 Watt SS power amp. Yeah, that might not be the most optimal match - but the volume attenuator on the preamp should keep the amp's input stage from getting overloaded and causing the sort of sonic issues you describe. So as @erik_squires mentioned, your main artifact of too much gain should just be noise floor.
The Cary is tubed - LOTS of 6SN7 - so you can tube roll to try and mitigate some of that sibilance. If you have Electro Harmonix 6SN7 in there now, then starting to replace them with any decent vintage tube should help a lot.
In modern era, preamps with gains over 20dB (almost always tube based 6SN7s or 12AX7s) are sort of an awkward fit.