Pat Metheny Bright Size Life and many other Pat's tracks involve hat sounds.
The arte del violine by Locatelli 3 cd...
Perfect to test any high frequencies...
And if you can the Four seasons by Vivaldi on Tacet...
here it is tube only TOP audiophile recording of violin...Stunning...
If your tweeter is good you will enter heaven...
Violin high notes are ideal test...Vibraphone and cymbals texture and decay in second for me...
1st, use CD's, something might be 'less than perfect' about your cartridge's many alignments. Then, compare your LP version to your CD version, gives you confidence, or helps you know re-adjustment(s) are needed.
Eurythmics, Sweet Dreams
Blue Nile, Walk Across the Rooftops
Duet: Barbra Streisand and Donna Summer: Enough is Enough, No More Tears
Andreas Vollenweider, White Winds
an inexpensive SPL Meter and Specific Test Frequencies, with tripod screw. on tripod, listening position, seated ear height
a CD with specific test frequencies, I use this one
tracks 9 to 38
expensive, I could help you find a copy.
now you can measure your highs, and also see how balanced all frequencies are at your spot, in that space.